• 专利标题:   Preparation of metal-doped graphene adsorbent for adsorbing decomposition product, involves adding graphene oxide and sodium nitrate, mixing hexachloroplatinic acid and aluminum chloride to obtain mixed solution, and ultrasonically treating.
  • 专利号:   CN115228436-A
  • 发明人:   LI W, CHEN L, LUO Y, GAO Y, WU X, WEI G, YI Q
  • 专利权人:   UNIV CHONGQING SCI TECHNOLOGY
  • 国际专利分类:   B01D053/02, B01J020/20, B01J020/30
  • 专利详细信息:   CN115228436-A 25 Oct 2022 B01J-020/20 202309 Chinese
  • 申请详细信息:   CN115228436-A CN10962460 11 Aug 2022
  • 优先权号:   CN10962460

▎ 摘  要

NOVELTY - Preparation of metal-doped graphene adsorbent involves (s1) adding graphene oxide and sodium nitrate in concentrated sulfuric acid with concentration of 98%, and adding potassium permanganate and stirring for 1-3 hours to obtain mixed solution (A), using hydrogen peroxide to oxidize mixed solution (A), washing product with distilled water, and drying to obtain nitrogen atom modified graphene, (s2) preparing nitrogen atom modified graphene-dimethylformamide solution with concentration of 0.025 mg/mL, soaking for 8 hours, performing ultrasonic oscillation for 1-2 hours, performing centrifugation, and using supernatant for later use, (s3) under argon atmosphere, mixing hexachloroplatinic acid and aluminum chloride, adding mixture in supernatant, and adjusting pH to be neutral by potassium hydroxide to obtain mixed solution (B), and (s4) carrying out ultrasonic treatment of mixed solution (B), heating mixed solution in microwave oven, washing with ethanol, and carrying out vacuum drying. USE - Preparation of metal-doped graphene adsorbent used for adsorbing decomposition product of sulfur hexafluoride (claimed). ADVANTAGE - The prepared graphene adsorbent has excellent electrical conductivity and adsorption performance.