• 专利标题:   Combustion synthesis of graphene powder by dry mixing magnesium powder and sugar powder in air atmosphere, subjecting mixed powder to high or normal pressure combustion synthesis reaction, acid washing, and washing by distilled water.
  • 专利号:   CN102826546-A, CN102826546-B
  • 发明人:   WANG L, FEI W
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102826546-A 19 Dec 2012 C01B-031/04 201337 Pages: 7 Chinese
  • 申请详细信息:   CN102826546-A CN10369707 28 Sep 2012
  • 优先权号:   CN10369707

▎ 摘  要

NOVELTY - Combustion synthesis of graphene powder by chemical co-precipitation method includes dry mixing magnesium powder and sugar powder in air atmosphere to obtain mixed powder; subjecting the mixed powder to high pressure combustion synthesis reaction or normal pressure combustion synthesis reaction; adding the mixed powder with hydrochloric acid; acid washing; washing by distilled water until washing liquid is neutral; and drying at normal pressure or vacuum drying. USE - Combustion synthesis of graphene powder (claimed). ADVANTAGE - The method uses raw materials having easy transportation and storage; saves energy; is simple and suitable for industrial production; has low cost; and provides graphene powder with small thickness. DETAILED DESCRIPTION - Combustion synthesis of graphene powder by chemical co-precipitation method comprises weighing 0.65-1 pt.wt. magnesium powder having purity of 95-99.99% and average particle diameter of 0.03-3 mm, and 1 pt.wt. sugar powder having purity of 95-99.9% and average particle diameter of 0.001-3 mm, where sugar is monosaccharide, disaccharide, oligosaccharide, or polysaccharide; adding into powder mixing machine; dry mixing in air atmosphere for 0.5-5 hours to obtain mixed powder; subjecting the mixed powder to high pressure combustion synthesis reaction or normal pressure combustion synthesis reaction; adding the mixed powder with 10-37% hydrochloric acid; acid washing until pH of washing liquid is less than 5; washing by distilled water until washing liquid is neutral; and drying at normal pressure or vacuum drying to obtain graphene powder.