• 专利标题:   Preparation of amine/amino functionalized graphene useful in e.g. biomedicine applications, involves mixing graphene oxide with organic solvent, adding aqueous solution of ammonia or amine compound and alkali solution, and neutralizing.
  • 专利号:   CN107043102-A, CN107043102-B
  • 发明人:   DAI Y, PANG H, ZHANG L, ZHONG B, SU Y, MAI Y, LIAO B
  • 专利权人:   GUANGDONG RES INST PETROCHEMICAL IND
  • 国际专利分类:   C01B032/184, C01B032/194
  • 专利详细信息:   CN107043102-A 15 Aug 2017 C01B-032/184 201774 Pages: 6 Chinese
  • 申请详细信息:   CN107043102-A CN10277063 25 Apr 2017
  • 优先权号:   CN10277063

▎ 摘  要

NOVELTY - The preparation method of amine/amino functionalized graphene involves adding graphene oxide to organic solvent and then ultrasonically processing, adding aqueous solution of ammonia or amine compound to the mixture and then stirring at 150-190 degrees C for 8-10 hours, filtering the mixture and then washing using water, adding alkali solution including halogen simple substance to the mixture and then performing Hofmann rearrangement reaction at 50-90 degrees C for 1-4 hours, neutralizing the mixture, and concentrating. USE - The method is useful for preparation of amine/amino functionalized graphene, which is useful in biomedicine and biochemical detection and treatment applications. ADVANTAGE - The method enables preparation of amine/amino functionalized graphene with excellent dispersibility and stability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for amine/amino functionalized graphene prepared by the method.