• 专利标题:   Preparing graphene-based lithium metal composite micro-rods comprises subjecting slurry to wet spinning, and coagulating, subjecting graphene oxide-based gel micro rod slurry to a hydrothermal reaction and filtering.
  • 专利号:   CN112643036-A
  • 发明人:   YU S, MA T, ZHANG L, LAN Y, YANG J
  • 专利权人:   UNIV CHINA SCI TECHNOLOGY
  • 国际专利分类:   B22F009/06, C01B032/184, H01M004/36, H01M004/38
  • 专利详细信息:   CN112643036-A 13 Apr 2021 B22F-009/06 202142 Pages: 21 Chinese
  • 申请详细信息:   CN112643036-A CN10958554 10 Oct 2019
  • 优先权号:   CN10958554

▎ 摘  要

NOVELTY - Preparing graphene-based lithium metal composite micro-rods comprises (i) subjecting slurry to wet spinning, and coagulating in a rotating coagulation bath to obtain a graphene oxide-based gel microrod slurry; where the slurry includes graphene oxide and water, (ii) subjecting the graphene oxide-based gel micro rod slurry to a hydrothermal reaction and filtering to obtain graphene-based micro rods, and (iii) adding graphene-based micron rod to molten lithium metal under a protective gas atmosphere, and stirring. USE - The graphene-based lithium metal composite micro-rods is used as lithium metal cathode active material without dendritic crystal generation in the battery circulation process. ADVANTAGE - The micro-rods has over-long cycle stability.