• 专利标题:   Lubricating plugging fluid loss agent for drilling fluid,comprises functional monomer,graphene oxide, water, oil phase dispersion medium, paraffin, composite emulsifier and initiator, which is prepared by adding all the raw materials, oil phase dispersion medium and paraffin into reaction kettle.
  • 专利号:   CN114686183-A
  • 发明人:   GE Q, WANG L, ZHAO H, ZHENG C, YAN B, WANG B, LIU J, LI X, LI Q
  • 专利权人:   DRILLING TECHNOLOGY RES INST SHENGLI OIL, SINOPEC SHENGLI OILFIELD ENG CO LTD, SINOPEC OILFIELD SERVICE CORP
  • 国际专利分类:   C09K008/03, C09K008/42
  • 专利详细信息:   CN114686183-A 01 Jul 2022 C09K-008/03 202277 Chinese
  • 申请详细信息:   CN114686183-A CN10859046 25 Dec 2020
  • 优先权号:   CN10859046

▎ 摘  要

NOVELTY - Lubricating plugging fluid loss agent for drilling fluid,comprises functional monomer, 0.6-0.8 pts.wt.graphene oxide, 80-100pts.wt.water, 70-80pts.wt. oil phase dispersion medium, 20-30 pts.wt. paraffin, 15-20 pts.wt.composite emulsifier and 1.0-1.5 pts.wt.initiator. USE - Lubricating plugging fluid loss agent for the drilling fluid. ADVANTAGE - The composition has wider particle size distribution range, effectively plugs microcracks with different sizes, forms a high-lubricity isolating membrane, has lubricating property, plugging property and filtrate loss reduction property, resists temperature up to 220 ℃ and NaCl to saturation, and has wide application prospect. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation method of the lubricating plugging fluid loss additive for the drilling fluid, involves adding 70-80 pts.wt. oil phase dispersion medium and 20-30 pts.wt. Paraffin into reaction kettle, slowly adding 15-20pts.wt. composite emulsifier under stirring condition of 80-100 r/min, and stirring for 40-60 min to obtain oil phase for later use, adding 80-100 pts.wt.water into another reaction kettle, starting stirring at rotating speed of 80-100 r/min for 30-40 min, then slowly adding 8-9 pts.wt.acrylic acid, 9-10pts.wt. acrylamide, 8-9 pts.wt.2-acrylamido-2-methylpropanesulfonic acid, 6-7pts.wt. styrene and 0.6-0.8 pts.wt.graphene oxide in sequence, adjusting pH value to 7-8, and stirring for 40-60 min to obtain water phase for later use;slowly adding water phase into oil phase, starting stirrer, regulating rotating speed to 120-150 r/min, stirring for 30-40 min, introducing nitrogen to remove oxygen for 30-50 min, adding 1.0-1.5 parts of an initiator, heating to 60-70 ℃, and polymerizing for 3-4 h to obtain final product.