• 专利标题:   Method for preparing transmission electron microscopy sample, involves transferring graphene to surface of material on which sample is prepared followed by hand grinding and obtaining sample containing graphene as protective layer.
  • 专利号:   CN108871890-A
  • 发明人:   GANG P, DOU Z, CHEN Z, LIU Z
  • 专利权人:   UNIV PEKING
  • 国际专利分类:   G01N001/28, G01N001/44
  • 专利详细信息:   CN108871890-A 23 Nov 2018 G01N-001/28 201902 Pages: 9 Chinese
  • 申请详细信息:   CN108871890-A CN10272364 29 Mar 2018
  • 优先权号:   CN10272364

▎ 摘  要

NOVELTY - A transmission electron microscopy sample preparation method involves transferring graphene to surface of material on which transmission electron microscopy sample is prepared or performing chemical vapor deposition, utilizing graphene to avoid surface damage and contamination caused by to-be-observed material, during sample preparation and performing hand grinding or ion beam thinning or using focused ion beam system for obtaining transmission electron microscopy sample containing graphene as protective layer, if the protective layer does not affect experimental observation, it is placed directly into the transmission electron microscope for observation, where the protective layer is removed by calcining at high temperature of 550 degrees C for 2 hours. USE - Method for preparing transmission electron microscopy sample. ADVANTAGE - The method enables preparing zero-damage transmission electron microscopy sample.