• 专利标题:   Preparing few-layer graphene by using graphite paper as anode and graphite plate as cathode, electrochemically stripping anode, washing product, drying, dispersing in solution comprising dispersant, mechanically stripping and spray drying.
  • 专利号:   CN110980707-A
  • 发明人:   DING G, ZHANG M, ZHOU J, FENG T, YAN Z, LIANG M, LI Y
  • 专利权人:   SHANGHAI XIWANG MATERIALS TECHNOLOGY CO
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN110980707-A 10 Apr 2020 C01B-032/19 202038 Pages: 12 Chinese
  • 申请详细信息:   CN110980707-A CN11253758 09 Dec 2019
  • 优先权号:   CN11253758

▎ 摘  要

NOVELTY - Method for preparing few-layer graphene by mechanical stripping involves using graphite paper as an anode and a graphite plate as a cathode, electrochemically stripping the anode in an electrolyte, filtering and separating to obtain an electrochemical stripping product, (ii) filtering and water-washing the electrochemical stripping product and drying to obtain electrochemically treated graphite, (iii) mixing a dispersant with water to obtain a mixed solution, uniformly dispersing the treated graphite in a mixed solution and carrying out mechanical stirring to obtain an electrochemically treated graphite aqueous dispersion and (iv) performing mechanical stripping on the dispersion to obtain a few-layer graphene aqueous dispersion and carrying out spray drying on the few-layer graphene aqueous dispersion. USE - The method is useful for preparing few-layer graphene. ADVANTAGE - The method does not require an organic solvent or an intercalation agent, adopts simple operation, is cost-effective and provides product with small radial size and few layers. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the few-layer graphene obtained by the method.