• 专利标题:   Graphene-chitosan Schiff base antibacterial aqueous coating comprises e.g. dispersing chitosan in dilute acetic acid, heating and stirring in a water bath, and adding hydrogen peroxide dropwise, cooling, slowly adding the photoinitiator, reducing the stirring rate, and continuously stirring.
  • 专利号:   CN115926509-A
  • 发明人:   LIANG B, PAN D
  • 专利权人:   SHENZHEN QIANHAI GRAPHENE IND CO LTD
  • 国际专利分类:   C09D004/02, C09D004/06, C09D005/14
  • 专利详细信息:   CN115926509-A 07 Apr 2023 C09D-004/06 202341 Chinese
  • 申请详细信息:   CN115926509-A CN11088635 07 Sep 2022
  • 优先权号:   CN11088635

▎ 摘  要

NOVELTY - Graphene-chitosan Schiff base antibacterial aqueous coating comprises (i) dispersing chitosan in dilute acetic acid, heating and stirring in a water bath, and adding hydrogen peroxide dropwise, cooling and adding absolute ethanol to precipitate out, (ii) mixing and dissolving water-soluble chitosan and vanillin in deionized water, heating and stirring in a water bath, cooling, filtering, adding ethanol to precipitate and washing for many times, and drying, (iii) dissolving aqueous chitosan Schiff base in 10 g deionized water, adding graphene, and ultrasonically dispersing, (iv) after allowing to stand polyurethane and deionized water for 12-20 hours, stirring for 25-80 minutes until completely dissolved to obtain a polyurethane dispersion, (v) adding the polyurethane dispersion into the stirring tank, then adding specific amount of water, and stirring for 10-40 minutes, slowly adding the photoinitiator, stirring, reducing the stirring rate, and continuously stirring. USE - The coating is useful in household appliances. ADVANTAGE - The coating: has excellent antibacterial effect to Escherichia coli, Staphylococcus aureus, Candida albicansand bacteria, antibacterial rate of more than 99% and strong antibacterial property and green health.