• 专利标题:   Preparation method for copper-capriblue metal nanosheet electrocatalyst, involves moving freeze-dried product into tube furnace, and calcined at predetermined value for predetermined value hours in ammonia gas atmosphere and add deionized water, isopropanol and naphthol solution to calcined product.
  • 专利号:   CN114086211-A, CN114086211-B
  • 发明人:   XU M, YE W
  • 专利权人:   UNIV HANGZHOU NORMAL
  • 国际专利分类:   B22F001/054, B22F001/12, B82Y030/00, B82Y040/00, C01B032/184, C25B001/01, C25B001/27, C25B011/091
  • 专利详细信息:   CN114086211-A 25 Feb 2022 C25B-011/091 202230 Chinese
  • 申请详细信息:   CN114086211-A CN11388312 22 Nov 2021
  • 优先权号:   CN11388312

▎ 摘  要

NOVELTY - The method involves dissolving the graphene oxide dispersion with a concentration of 2 to 3 g/L in deionized water to form a first solution. The volume ratio of graphene oxide dispersion to deionized water is 1:0.3\=0.8. The copper chloride dihydrate is added to the first solution, and the second solution is formed by ultrasonicating for 20-60 min according to the addition ratio of 10-100 grams per liter. The freeze-dried product is moved into a tube furnace, and calcined at 600-800degrees for 2-4 hours in an ammonia gas atmosphere. The deionized water, isopropanol, and naphthol solution are added to the calcined product successively. The addition ratio follows 150-200 ml of deionized water, 50-80 ml of isopropanol, 10-15 ml of naphthol solution per gram of product, and ultrasonic for 20-60 min to obtain the copper-capriblue metal nanosheet electrocatalyst. USE - Preparation method for copper-capriblue metal nanosheet electrocatalyst. ADVANTAGE - The synthesis method provides simple process, low energy consumption, mild conditions, good product appearance and the like, and is suitable for large-scale production applications. DESCRIPTION OF DRAWING(S) - The drawing shows a graphical representation of stability test of copper-capriblue metal nanosheet electrocatalyst (Drawing includes non-English language text).