• 专利标题:   Preparation of loading platinum nanoparticle on graphene comprises taking restored graphene to ultrasonic disperse in glycol solution, adding glycol solution of 1-pyrene methylamine, adding chloroplatinic acid glycol solution, and reacting.
  • 专利号:   CN102120186-A, CN102120186-B
  • 发明人:   SHI Y, LI W, QIU H, PAN L, ZHAI D, PANG H
  • 专利权人:   UNIV NANJING
  • 国际专利分类:   B01J031/28, G01N021/65, H01M004/92
  • 专利详细信息:   CN102120186-A 13 Jul 2011 B01J-031/28 201169 Pages: 7 Chinese
  • 申请详细信息:   CN102120186-A CN10552955 22 Nov 2010
  • 优先权号:   CN10552955

▎ 摘  要

NOVELTY - Preparation of loading platinum nanoparticle on graphene comprises taking restored graphene to ultrasonic disperse in glycol solution, adding glycol solution of 1-pyrene methylamine, and stirring for 20-120 minutes to self-assemble 1-pyrene methylamine on surface of the graphene; and adding 0.048 M chloroplatinic acid glycol solution (Nml), adjusting pH of glycol solution to 8-9 by 0.1 M sodium hydroxide, stirring, reacting for 2 hours in oil bath at 160 degrees C to obtain high-density loading platinum nanoparticle on graphene, cleaning and drying in freeze mode. USE - Method of preparation of loading platinum nanoparticle on graphene (claimed). DETAILED DESCRIPTION - Preparation of loading platinum nanoparticle on graphene comprises taking restored graphene to ultrasonic disperse in glycol solution, adding glycol solution of 1-pyrene methylamine, with ratio (mg:ml:ml) of graphene, glycol and glycol solution of 1-pyrene methylamine of 1:8-20:1-1.5, and concentration of glycol solution of 1-pyrene methylamine at 10-3 M, and stirring for 20-120 minutes to self-assemble 1-pyrene methylamine on surface of the graphene; and adding 0.048 M chloroplatinic acid glycol solution (Nml), with ratio (mg: ml) of graphene and Nml at 1:0.8-1.5, adjusting pH of glycol solution to 8-9 by 0.1 M sodium hydroxide, stirring, reacting for 2 hours in oil bath at 160 degrees C to obtain high-density loading platinum nanoparticle on graphene, cleaning and drying in freeze mode. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic diagram of the preparation of loading platinum nanoparticle on graphene.