• 专利标题:   Graphene/metal phthalocyanine composite material preparation includes placing graphene into organic solvent, ultrasonic dispersing, adding precursor and metal salt, and microwave reacting.
  • 专利号:   CN102863449-A
  • 发明人:   LIU L, DAI W, BU Y, ZUO X
  • 专利权人:   UNIV CAPITAL NORMAL
  • 国际专利分类:   C07D487/22
  • 专利详细信息:   CN102863449-A 09 Jan 2013 C07D-487/22 201344 Pages: 9 Chinese
  • 申请详细信息:   CN102863449-A CN10353304 20 Sep 2012
  • 优先权号:   CN10353304

▎ 摘  要

NOVELTY - A graphene/metal phthalocyanine composite material is prepared by placing graphene into organic solvent; ultrasonic dispersing for 10-30 minutes to obtain graphene oxide suspension solution pool; adding precursor and metal salt to filtrate; fully mixing and adding water to the obtained graphite alkene suspending liquid and metal salt mixture; microwave reacting at 90-160 degrees C for 5-50 minutes; and refluxing, filtering, pouring anhydrous ethanol, vacuum drying at 40-100 degrees C for 6-30 hours to obtain black powdered product. USE - Microwave synthesis for preparing graphene/metal phthalocyanine composite material (claimed). ADVANTAGE - The method has simple operation, and fast and mild reaction. DETAILED DESCRIPTION - Microwave synthesis for preparing graphene/metal phthalocyanine composite material comprises placing graphene into organic solvent (10 mg graphene/ml solvent); ultrasonic dispersing for 10-30 minutes to obtain graphene oxide suspension solution pool; adding precursor and metal salt to filtrate at a mole ratio of 2-9:1; fully mixing, adding water to the obtained graphite alkene suspending liquid and metal salt mixture; microwave reacting at 90-160 degrees C for 5-50 minutes; and refluxing, filtering, pouring anhydrous ethanol, vacuum drying at 40-100 degrees C for 6-30 hours to obtain black powdered product, graphite/metal phthalocyanine composite material.