• 专利标题:   Preparing magnetic surface molecular imprinting electrochemical sensor useful in tetrabromobisphenol recognition and detection, comprises introducing reversible addition-fragmentation chain transfer reagent into azidefunctionalized magnetic carrier, polymerizing and modifying glassy carbon electrode.
  • 专利号:   CN114644737-A
  • 发明人:   FEI G, WANG H, AN J, ZHAO Z, WANG P, ZHENG R, ZHU Y, SHAO Y
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   C08F222/14, C08F226/06, C08F283/00, C08F292/00, C08J009/26, G01N027/30
  • 专利详细信息:   CN114644737-A 21 Jun 2022 C08F-292/00 202290 Chinese
  • 申请详细信息:   CN114644737-A CN10259030 16 Mar 2022
  • 优先权号:   CN10259030

▎ 摘  要

NOVELTY - Preparing magnetic surface molecular imprinting electrochemical sensor comprises (i) introducing the magnetic ferroso ferric oxide nano-particle into the graphene oxide to prepare magnetic oxidation graphene the nano material; (ii) using dopamine to modify the magnetic oxidation graphene the nano material to obtain a polydopamine-modified magnetic nano-microsphere; (iii) subjecting the polydopamine-modified magnetic nano-microspheres to surface azide treatment to obtain azide-functionalized magnetic carriers; (iv) introducing the reversible addition-fragmentation chain transfer reagent into the azide-functionalized magnetic carrier by click chemistry, and polymerizing to obtain a magnetic surface molecularly imprinted polymer; and (v) modifying the glassy carbon electrode by the magnetic surface molecularly imprinted polymer. USE - The method is useful for preparing magnetic surface molecular imprinting electrochemical sensor is useful in recognition and detection of tetrabromobisphenol A in an environmental system (claimed). ADVANTAGE - The method prepares magnetic surface molecular imprinting electrochemical sensor with rich and template molecule mass transfer rate thus detects the tetrabromobisphenol A in the sample to be tested with simple principle, readily available raw material cost without any large instrument by realizing the high sensitivity and specificity detection of tetrafluoromethane A. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for magnetic surface molecular imprinting electrochemical sensor, prepared as mentioned above.