• 专利标题:   Preparation of amorphous iron vanadate/bismuth vanadate/graphene composite photocatalyst for advanced treatment of photocatalytic reduction of chromium (VI) and/or chromium-containing wastewater, involves preparing bismuth nitrate solution.
  • 专利号:   CN108404926-A
  • 发明人:   HUANG Z, DAI X, CHEN X, YE J, HU Z
  • 专利权人:   UNIV SOUTH CHINA AGRIC
  • 国际专利分类:   B01J023/847, B01J035/02, B82Y020/00, B82Y030/00, B82Y040/00, C02F001/30, C02F001/70, C02F101/22
  • 专利详细信息:   CN108404926-A 17 Aug 2018 B01J-023/847 201861 Pages: 11 Chinese
  • 申请详细信息:   CN108404926-A CN10146379 12 Feb 2018
  • 优先权号:   CN10146379

▎ 摘  要

NOVELTY - An amorphous iron vanadate/bismuth vanadate/graphene composite photocatalyst is prepared by preparing bismuth nitrate glycerol solution, adding graphene powder, ultrasonicating for 10-15 minutes, preparing ammonium metavanadate aqueous solution and ferric nitrate solution, mixing ferric nitrate solution and prepared bismuth nitrate glycerol solution, clarifying, adding ammonium metavanadate aqueous solution, stirring for 15-30 minutes, adjusting pH value to 4-7 to obtain precursor solution, standing and aging for 1-2 hours, carrying out hydrothermal reaction for 10-20 hours at 158-162 degrees C, obtaining suspension, standing for 10-30 minutes, removing 1/2 volume of supernatant, adding ascorbic acid solution, standing for 0.5-1 hour under inert gas protection, alternatively washing 3 times with anhydrous ethanol and deionized water, and drying for 10-20 hours at 60 degrees C. USE - Method for preparing amorphous iron vanadate/bismuth vanadate/graphene composite photocatalyst for advanced treatment of photocatalytic reduction of chromium (VI) and/or chromium-containing wastewater (claimed). ADVANTAGE - The product has large specific surface area.