• 专利标题:   Preparation of water-soluble graphene by double-graphite electrode electric field driving by dissolving hydrate containing EDTA salt and metal hydroxide in water, putting double-graphite electrode, starting to react, dispersing and drying.
  • 专利号:   CN112225206-A
  • 发明人:   LI L, ZHANG D
  • 专利权人:   UNIV SHAANXI TECHNOLOGY
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN112225206-A 15 Jan 2021 C01B-032/19 202117 Pages: 11 Chinese
  • 申请详细信息:   CN112225206-A CN11128247 20 Oct 2020
  • 优先权号:   CN11128247

▎ 摘  要

NOVELTY - Preparation of water-soluble graphene by double-graphite electrode electric field driving comprises dissolving hydrate containing EDTA salt and metal hydroxide in deionized water to form electrolyte, putting double-graphite electrode in electrolyte, accessing square wave voltage, starting to react until double-graphite electrode is peeled off, cleaning electrolytic solution after multiple reactions, ultrasonically dispersing to obtain water-soluble graphene dispersion liquid, and drying dispersion liquid to obtain water-soluble graphene nanosheet powder. USE - The method is for preparing water-soluble graphene by double-graphite electrode electric field driving. ADVANTAGE - The method uses double-graphite foil as anode and cathode which reduces use of noble metal electrode, reduces cost, improves yield, uses common beaker or glassware as simple device, is green and environment-friendly, and has short operation time and convenient operation, and is simple and easy to amplify. The graphene has high quality, good conductivity and excellent dispersibility in water.