• 专利标题:   Preparing small sized graphene comprises e.g. mixing graphite powder with solvent, mixing, starting cooling system to maintain constant temperature, stirring at high speed, allowing to stand, centrifuging, and collecting supernatant.
  • 专利号:   CN104003375-A, CN104003375-B
  • 发明人:   LIU L, ZHANG X, MA S, SHEN Z
  • 专利权人:   UNIV BEIJING AERONAUTICS ASTRONAUTICS
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B031/04
  • 专利详细信息:   CN104003375-A 27 Aug 2014 C01B-031/04 201477 Pages: 10 Chinese
  • 申请详细信息:   CN104003375-A CN10186353 05 May 2014
  • 优先权号:   CN10186353

▎ 摘  要

NOVELTY - Preparing small sized graphene comprises (a) mixing graphite powder with a solvent to obtain graphite mixed solution, (b) transferring the solution into a container, simultaneously mixing by a mixer equipped with stator and rotor, where the rotor is set with a homogenizing head below the liquid level, (c) starting a cooling system to maintain a constant temperature, and stirring at a high speed and (d) allowing to stand, centrifugally separating, removing the particles, which are not completely stripped, and collecting supernatant to obtain stable small sized graphene dispersion liquid. USE - The method is useful for preparing small sized graphene (claimed). ADVANTAGE - The method: uses a rotor for high speed rotation to drive fluid with high speed to produce high speed gradient, and high cutting force; carries out refining and separation of graphite sheet by high speed impinging of high speed fluid and lug boss stator hole wall; has less investment for devices; is economical, simple and easy; has high yield; and is suitable for laboratory and large-scale industrial production. The graphene product has centralized distribution with single ratio.