• 专利标题:   Modifying carbon fiber supporting epoxy resin used as base material in chemical process device e.g. adding diethylenetriamine, 1-ethyl-carbodiimide hydrochloride and N-hydroxysuccinimide, mixing and stirring organic phase, and adding alkaline solution and reacting.
  • 专利号:   CN115558242-A
  • 发明人:   GUO Z, CHEN L, HE L, LIU D
  • 专利权人:   HARBIN INST TECHNOLOGY SHENZHEN GRADUATE, SHENZHEN JINU INNOVATION TECHNOLOGY CO
  • 国际专利分类:   C08G059/06, C08K007/06, C08L001/02, C08L013/00, C08L015/00, C08L063/02
  • 专利详细信息:   CN115558242-A 03 Jan 2023 C08L-063/02 202317 Chinese
  • 申请详细信息:   CN115558242-A CN10747836 02 Jul 2021
  • 优先权号:   CN10747836

▎ 摘  要

NOVELTY - Modifying carbon fiber supporting epoxy resin, comprises (a) mixing epichlorohydrin with bisphenol A and catalyst promoter to form a mixed solution, adding alkaline solution in the mixed solution and reacting to obtain bisphenol A epoxy resin reaction crude liquid, (b) mixing carboxy-terminated nitrile rubber and hydroxy-terminated nitrile rubber with an organic solvent at 70-90℃, adding phosphoric acid solution and reacting, washing and separating the reaction product, and separating organic phase, (c) adding diethylenetriamine, 1-ethyl-carbodiimide hydrochloride and N-hydroxysuccinimide to the nanocellulose solution, and stirring at room temperature, obtaining graphene oxide grafts nanocellulose, and (d) mixing and stirring the organic phase obtained by the bisphenol A epoxy resin reaction thick liquid, graphene oxide grafted nanocellulose, and adding alkaline solution to react, through separation, washing and drying. USE - The method is useful for modification of carbon fiber matched epoxy resin used as base material in chemical process device in adhesive, and coating. ADVANTAGE - The method improves each intensity parameter of the prepared material.