• 专利标题:   Electrode material for use in 3D petal graphite alkene-polyaniline super capacitor, is obtained by functionalizing graphene oxide precursor to prepare amino triazine functionalized graphene oxide.
  • 专利号:   CN104064363-A, CN104064363-B
  • 发明人:   GUANG S, KE F, LIU Y, XU H
  • 专利权人:   UNIV DONGHUA
  • 国际专利分类:   H01G011/32, H01G011/48, H01G011/86
  • 专利详细信息:   CN104064363-A 24 Sep 2014 H01G-011/32 201501 Pages: 11 Chinese
  • 申请详细信息:   CN104064363-A CN10216059 20 May 2014
  • 优先权号:   CN10216059

▎ 摘  要

NOVELTY - An electrode material is obtained by functionalizing graphene oxide precursor to prepare amino triazine functionalized graphene oxide(ATRGO) followed by carrying out aniline monomer in-situ oxidation process of amino triazine functionalized graphene oxide after freeze-drying to obtain a finished product. USE - Electrode material for use in a 3D petal graphite alkene-polyaniline super capacitor. ADVANTAGE - The electrode material can be prepared in an eco-friendly manner. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing an electrode material, which involves preparing mono-dispersed graphene oxide, mixing oxidized graphite alkene with sodium bicarbonate and cooling with 1,3, 4-trichloro-2,4,6-triazine at 0 degrees C for 3-4 hours, adding para-phenylene diamine at room temperature for 3-4 hours to obtain a mixture solution, filtering, washing and drying the mixture solution under vacuum to obtain ATRGO, subjecting the ATRGO to ultrasonic dispersion with hydrochloric acid and initiator at 0 degrees C for 12-24 hours followed by centrifuging, filtering, washing, freezing and drying to obtain 3D-petal graphite alkene- polyaniline super capacitor electrode material, where the graphene oxide, sodium bicarbonate, 1,3, 4-trichloro-2, 4,6-triazine, p-phenylenediamine to ratio of 400:60-65:15-17:60-68 mmol, the hydrochloric acid and ATRGO to mass ratio of 1:1-100:1, the triazine functionalized graphite and aniline to mass ratio of 1:1-1:300, the nitiator and aniline to mass ratio of 1:1-1:10.