• 专利标题:   Preparing mesoporous material by microwave-assisted loaded nano-silver oxide comprises e.g. mixing graphene oxide and furfuryl alcohol, selecting mesoporous material to be treated, adding solution of hydrogen chloride, drying and spraying.
  • 专利号:   CN106279471-A
  • 发明人:   LI H
  • 专利权人:   QINGDAO LANNONGGU AGRIC PROD RES DEV
  • 国际专利分类:   C08F010/00, C08F004/02, C08F004/10, C08F004/18
  • 专利详细信息:   CN106279471-A 04 Jan 2017 C08F-004/02 201721 Pages: 5 Chinese
  • 申请详细信息:   CN106279471-A CN10285589 29 May 2015
  • 优先权号:   CN10285589

▎ 摘  要

NOVELTY - Preparing mesoporous material by microwave-assisted loaded nano-silver oxide comprises e.g. (i) mixing zinc acetate dihydrate, loading solution, silver nitrate, adding 3 times the volume of deionized water, (ii) mixing graphene oxide and furfuryl alcohol, (iii) selecting mesoporous material to be treated, placing in solution A, soaking, (iv) drying and impregnating into solution B, adding solution of hydrogen chloride, and (v) passing deep impregnated mesoporous material through nitrogen, drying and spraying 5-6 wt.% titanium dioxide catalyst on a surface, and drying. USE - The method is useful for preparing mesoporous material by microwave-assisted loaded nano-silver oxide (claimed). ADVANTAGE - The method has improved yield. DETAILED DESCRIPTION - Preparing mesoporous material by microwave-assisted loaded nano-silver oxide comprises (i) mixing zinc acetate dihydrate, loading solution, silver nitrate in a mass ratio of 2:3:5, adding 3 times the volume of deionized water, stirring, filtering metal ion saturated solution at room temperature, storing saturated solution in ice-water bath at 0-5 degrees C to obtain solution A, (ii) mixing graphene oxide and furfuryl alcohol in a weight ratio of 2:7 under ultrasonic power of 500-700 W under the conditions of ultrasonic treatment for 3-4 hours to obtain solution B, (iii) selecting the mesoporous material to be treated, placing in solution A at constant temperature 5 degrees C, soaking for 50-60 minutes, (iv) after the initial impregnation of the mesoporous material at room temperature, drying and impregnating into solution B under the conditions of ultrasonic power 500-700 W and ultrasonic treatment for 1.2-1.5 hours, where mass ratio between hydrogen chloride and silver nitrate is 2:1, adding solution of hydrogen chloride having concentration 0.8 mol/L(-1), and (v) passing deep impregnated mesoporous material through nitrogen, drying and spraying 5-6 wt.% titanium dioxide catalyst on a surface, and drying at room temperature for 24 hours.