• 专利标题:   Preparing hydrophobic film with low water absorption comprises e.g. drying corn starch, placing in oil bath, adding vinyltriethoxysilane and stearic acid, activating, and dissolving soybean isolated protein and urea in deionized water.
  • 专利号:   CN112266492-A
  • 发明人:   LI W, YANG Y
  • 专利权人:   BENGBU WEIGUANG PLASTIC RUBBER PROD CO
  • 国际专利分类:   C08J005/18, C08K013/06, C08K003/04, C08K003/22, C08K005/09, C08K005/1515, C08K005/21, C08K007/28, C08K009/04, C08L003/02, C08L063/00, C08L089/00
  • 专利详细信息:   CN112266492-A 26 Jan 2021 C08J-005/18 202124 Pages: 6 Chinese
  • 申请详细信息:   CN112266492-A CN11315561 21 Nov 2020
  • 优先权号:   CN11315561

▎ 摘  要

NOVELTY - Preparing hydrophobic film with low water absorption comprises (i) drying 20-30 pts. wt. corn starch at 110-120 degrees C for 1-2 hours, placing in oil bath at 100-105 degrees C, adding 0.6-0.9 pts. wt. silane coupling agent A-151 (vinyltriethoxysilane) and 0.6-0.9 pts. wt. stearic acid, and activating for 10-20 minutes to obtain hydrophobized corn starch, (ii) dissolving 20-30 pts. wt. soybean isolated protein and 10-15 pts. wt. urea in 250-280 pts. wt. deionized water, adjusting pH using sodium hydroxide solution, adding 5-7.5 pts. wt. epoxy oleic acid, 5-7.5 pts. wt. emulsified epoxy resin, and reacting to obtain compound modified soybean protein emulsion, and (iii) mixing hydrophobized corn starch and modified soybean protein emulsion, adding 2-3 pts. wt. reduced graphene oxide solution, 1-2 pts. wt. modified hollow glass beads and 1-2 pts. wt. surface-treated nano antimony tin oxide, casting into polytetrafluoroethylene mold, and drying in oven at 45-50 degrees C for 20-24 hours to obtain film. USE - The method is useful for preparing hydrophobic film with low water absorption.