• 专利标题:   Preparation of patterned graphene thin film on electrospun fiber network by pretreating glass, electrospinning using polyacrylonitrile N,N-dimethyl formamide solution, immersing in graphene oxide aqueous solution using Czochralski method.
  • 专利号:   CN107365090-A
  • 发明人:   FENG Z, LI J, NIE X, SHI C, ZHAO B
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   C03C017/42
  • 专利详细信息:   CN107365090-A 21 Nov 2017 C03C-017/42 201802 Pages: 9 Chinese
  • 申请详细信息:   CN107365090-A CN10320127 13 May 2016
  • 优先权号:   CN10320127

▎ 摘  要

NOVELTY - Preparation of a patterned graphene thin film on an electrospun fiber network comprises pretreating a glass substrate by immersing in a mixed solution for 0.5-4 hours, washing in ethanol and ultrapure water, placing in3-aminopropyltriethoxysilane toluene solution for 0.5 hours, and washing with toluene, ethanol, and ultrapure water; electrospinning using polyacrylonitrile N,N-dimethyl formamide solution; immersing in 0.1-2 mg/mL graphene oxide aqueous solution for 200-700 nm/seconds, and using Czochralski method; and placing the glass substrate in a vacuum environment using hydrazine hydrate. USE - Method for preparing patterned graphene thin film on an electrospun fiber network. ADVANTAGE - The method is simple to operate and has low cost. DETAILED DESCRIPTION - Preparation of a patterned graphene thin film on an electrospun fiber network comprises: (A) pretreating a glass substrate by immersing in a mixed solution for 0.5-4 hours, washing in ethanol and ultrapure water, placing in 3 vol.% 3-aminopropyltriethoxysilane toluene solution for 0.5 hours, and washing with toluene, ethanol, and ultrapure water; (B) electrospinning the glass substrate as carrier using polyacrylonitrile N,N-dimethyl formamide solution at 14-16 kV for 0.8-1.2 mL/hour; (C) immersing the electro-spun fiber-covered glass substrate in 0.1-2 mg/mL graphene oxide aqueous solution for 200-700 nm/seconds, and using Czochralski method to obtain patterned graphene oxide film; and (D) placing the glass substrate in a vacuum environment using hydrazine hydrate.