• 专利标题:   Preparing graphene involves adding graphite oxide to ethanol, ultrasonically treating mixture, mixing magnesium powder with liquid, ultrasonically stirring liquid, vacuum drying slurry, sintering, crushing, and extracting material.
  • 专利号:   CN104609407-A
  • 发明人:   LIU Y, ZENG X, YUAN Q
  • 专利权人:   UNIV NANCHANG
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104609407-A 13 May 2015 C01B-031/04 201556 Pages: 6 Chinese
  • 申请详细信息:   CN104609407-A CN10026193 20 Jan 2015
  • 优先权号:   CN10026193

▎ 摘  要

NOVELTY - The preparation method of graphene by magnesium-reduction of graphene oxide involves adding graphite oxide to ethanol solution, ultrasonically treating mixture to obtain 0.1-10 mg/ml graphene oxide-ethanol mixed liquid, mixing magnesium powder with mixed liquid, ultrasonically stirring liquid to obtain uniformly dispersed slurry, filtering and vacuum drying slurry at 1-100 MPa to obtain compact material, sintering compact material at 400-600 degrees C for 2 hours, crushing compact material, and extracting crushed material with hydrochloric acid. USE - The method is useful for preparation of graphene by magnesium-reduction of graphene oxide (claimed). ADVANTAGE - The method ensures simple, economical, industrial and environmentally-friendly preparation of graphene without using toxic reagent in short time at low temperature.