• 专利标题:   Preparing chitosan/aminated graphene oxide nano composite membrane adsorbent comprises adding graphite oxide, stirring uniformly, dispersing, centrifuging, heating, reacting, dialyzing, scraping a film, washing to neutrality and drying.
  • 专利号:   CN110586043-A
  • 发明人:   DING C, LI L, ZHANG Y
  • 专利权人:   UNIV TIANJIN POLYTECHNIC
  • 国际专利分类:   B01J020/24, B01J020/28, B01J020/30, C02F001/28, C02F101/20
  • 专利详细信息:   CN110586043-A 20 Dec 2019 B01J-020/24 202005 Pages: 7 Chinese
  • 申请详细信息:   CN110586043-A CN10878706 18 Sep 2019
  • 优先权号:   CN10878706

▎ 摘  要

NOVELTY - Preparing chitosan/aminated graphene oxide nano composite membrane adsorbent comprises (i) adding 100 mg graphite oxide into 100 ml distilled water, stirring uniformly, dispersing ultrasonically for a specific time, centrifuging in a high-speed centrifuge and taking a specific amount of supernatant; (ii) adding a specific amount of ethylenediamine into graphene oxide solution under stirring, heating the mixed solution under magnetic stirring, reacting and dialyzing the mixed solution for 24 hours to a conductivity of 0; (iii) adding the mixed solution into chitosan acetic acid solution with a specific mass fraction, mechanically stirring for 6 hours, allowing to stand and defoaming, scraping a film by casting method, drying and placing in alkaline solution for 30 minutes; and (iv) repeatedly washing composite film to neutrality with a large amount of distilled water and drying the composite film in a vacuum drying box. USE - The method is useful for preparing chitosan/aminated graphene oxide nano composite membrane adsorbent. ADVANTAGE - The method is simple, the raw materials are environmentally friendly and the adsorption effect of the product on cupric ion is enhanced.