• 专利标题:   Preparing graphitic alkenyl nano-borate composite material involves adding graphene oxide and water and dissolving to obtain solution, mixing with alkyl phenol and N,N-dimethyl acetamide and dispersing to obtain graphene oxide solution.
  • 专利号:   CN107460021-A
  • 发明人:   CHEN W, CHEN Y, LIN Z, PAN M, YANG H, YAO Y
  • 专利权人:   UNIV QUANZHOU NORMAL, XIAMEN 6C TECHNOLOGY CO LTD
  • 国际专利分类:   C10M125/26, C10M177/00, C10N020/06, C10N030/06
  • 专利详细信息:   CN107460021-A 12 Dec 2017 C10M-125/26 201803 Pages: 7 Chinese
  • 申请详细信息:   CN107460021-A CN10667622 07 Aug 2017
  • 优先权号:   CN10667622

▎ 摘  要

NOVELTY - Preparing graphitic alkenyl nano-borate composite material involves adding 1 pts. wt. graphene oxide and 1000-3000 pts. wt. water and dissolving to obtain solution, mixing solution with 1-60 pts. wt. alkyl phenol and N,N-dimethyl acetamide and ultrasonically dispersing for 2-3 hours to obtain 0.3-1 milligram/milliliter graphene oxide solution. The reaction mixture is stirred at 80 degrees C, followed by the addition of 20-30 pts. wt. sodium borohydride and sodium mixed solution and stirred for 1-2 hours. 10-1000 pts. wt. hexadecyl calcium borate and nano-cerium borate are stirred for 10-15 hours. USE - Method for preparing graphitic alkenyl nano-borate composite material (claimed). ADVANTAGE - The method enables to prepare graphitic alkenyl nano-borate composite material in simple manner which has mild reaction condition, is easy to realize and convenient to operate. DETAILED DESCRIPTION - Preparing graphitic alkenyl nano-borate composite material involves adding 1 pts. wt. graphene oxide and 1000-3000 pts. wt. water and dissolving to obtain solution, mixing solution with 1-60 pts. wt. alkyl phenol and N,N-dimethyl acetamide and ultrasonically dispersing for 2-3 hours to obtain 0.3-1 milligram/milliliter graphene oxide solution. The reaction mixture is stirred at 80 degrees C, followed by the addition of 20-30 pts. wt. sodium borohydride and sodium mixed solution and stirred for 1-2 hours. 10-1000 pts. wt. hexadecyl calcium borate and nano-cerium borate, are mixed and stirred for 10-15 hours. The reaction mixture is stirred and refluxed on oil bath for 5-20 hours at certain temperature. The mixture is hot filtered, washed and dried to obtain desired product.