• 专利标题:   Preparation of magnetic graphene oxide involves taking graphene oxide and glycol solution, stirring, adding iron(III) chloride hexahydrate and sodium acetate trihydrate, stirring, reacting, filtering, taking filter cake, and washing.
  • 专利号:   CN106362692-A
  • 发明人:   HU D, LIAO W, LIU J, ZHOU Y
  • 专利权人:   SHENZHEN NTEK TESTING TECHNOLOGY CO LTD
  • 国际专利分类:   B01J020/20, B01J020/28, B01J020/281, B01J020/30, G01N030/02
  • 专利详细信息:   CN106362692-A 01 Feb 2017 B01J-020/20 201725 Pages: 15 Chinese
  • 申请详细信息:   CN106362692-A CN10984065 07 Nov 2016
  • 优先权号:   CN10984065

▎ 摘  要

NOVELTY - A magnetic graphene oxide is prepared by taking graphene oxide and glycol solution, stirring, adding iron(III) chloride hexahydrate and sodium acetate trihydrate, stirring, reacting, filtering, taking filter cake, washing with water and ethanol, and drying. USE - Method for preparing magnetic graphene oxide (claimed). ADVANTAGE - The method is simple, low-cost and environment-friendly. The product has large specific surface area, strong absorbing ability and enriches water phthalates substances. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for phthalate substance content measurement method comprising taking 50-100 mL sample, adding 0.2-0.5 g magnetic graphene oxide, ultrasonic dispersing for 60 plus minus 10 minutes, performing magnetic separation, removing supernatant, leaving lower layer mixed liquid, adding 2 plus minus 1 mL dichloromethane, ultrasonically processing for 60 plus minus 10 minutes, performing magnetic separation, removing supernatant, leaving lower layer mixed liquid, filtering, and carrying out GC-MS analysis.