• 专利标题:   Preparation of graphene film involves plating carbon-containing metal, forming metal film, providing obtained silicon substrate, plating with metal film in vacuum annealing furnace and etching silicon substrate.
  • 专利号:   CN101988184-A, CN101988184-B
  • 发明人:   LIU N, FU L, LIU Z
  • 专利权人:   UNIV PEKING
  • 国际专利分类:   C23C014/16, C23C014/24, C23C014/58
  • 专利详细信息:   CN101988184-A 23 Mar 2011 C23C-014/24 201136 Pages: 9 Chinese
  • 申请详细信息:   CN101988184-A CN10090360 06 Aug 2009
  • 优先权号:   CN10090360

▎ 摘  要

NOVELTY - A carbon-containing metal is plated to silicon substrate having thermal oxidation layer, and metal film is formed to obtain silicon substrate. The obtained silicon substrate is provided and plated with metal film into a vacuum annealing furnace, annealing is carried out at 900-1100 degrees C for 5-100 minutes and pressure of 10-4-10-2 Pa to obtain sample comprising graphene, metal film, thermal oxidation layer and silicon substrate. The obtained silicon substrate is etched to obtain graphene film. USE - Preparation of graphene film. ADVANTAGE - The method efficiently provides graphene film having uniformly dispersed carbon and large surface area, by a simple process.