• 专利标题:   Preparing layered flame-retardant material involves dispersing N,N-dimethylformamide and graphene oxide ultrasonically, adding flame retardant, ultrasonically dispersing it, and subjecting it to centrifugation, washing and drying.
  • 专利号:   CN112920564-A
  • 发明人:   CHEN B, LI Z, ZHAO T, WANG Z, LI J, MAO J
  • 专利权人:   UNIV XIHUA
  • 国际专利分类:   C08K003/04, C08L067/02, C08L091/06
  • 专利详细信息:   CN112920564-A 08 Jun 2021 C08L-067/02 202160 Pages: 18 Chinese
  • 申请详细信息:   CN112920564-A CN10123356 29 Jan 2021
  • 优先权号:   CN10123356

▎ 摘  要

NOVELTY - Preparing a layered flame-retardant material involves dispersing N,N-dimethylformamide and graphene oxide ultrasonically at 20-40 degrees C for 20-40 minutes, adding intumescent flame retardant, ultrasonically dispersing it at 20-40 degrees C for 20-40 minutes, and then subjecting it to centrifugation, washing and drying to obtain modified flame retardant I. The N,N-dimethylformamide and graphene oxide are dispersed ultrasonically at 20-40 degrees C for 20-40 minutes, intumescent flame retardant is added and ultrasonically dispersed at 20-40 degrees C for 20-40 minutes, dicyclohexylcarbodiimide is added and mechanically stirred for 22-24 hours at 40-60 degrees C in water bath, and then centrifuged, cleaned and dried to obtain modified flame retardant II. The modified flame retardant I or modified flame retardant II are combined with the intumescent flame retardant and polybutylene terephthalate at 70-90 degrees C, dried for 8-12 hours, mixed, and added with liquid paraffin and antioxidant at same time. USE - Method for preparing a layered flame-retardant material. ADVANTAGE - The method enables to prepare a layered flame-retardant material, which improves flame retardant performance of flame retardant material, and effectively solves problem of poor flame retardant performance, easy dripping, and reduced mechanical property. DETAILED DESCRIPTION - Preparing a layered flame-retardant material involves dispersing N,N-dimethylformamide and graphene oxide ultrasonically at 20-40 degrees C for 20-40 minutes, adding intumescent flame retardant, ultrasonically dispersing it at 20-40 degrees C for 20-40 minutes, and then subjecting it to centrifugation, washing and drying to obtain modified flame retardant I. The N,N-dimethylformamide and graphene oxide are dispersed ultrasonically at 20-40 degrees C for 20-40 minutes, intumescent flame retardant is added and ultrasonically dispersed at 20-40 degrees C for 20-40 minutes, dicyclohexylcarbodiimide is added and mechanically stirred for 22-24 hours at 40-60 degrees C in water bath, and then centrifuged, cleaned and dried to obtain modified flame retardant II. The modified flame retardant I or modified flame retardant II are combined with the intumescent flame retardant and polybutylene terephthalate at 70-90 degrees C, dried for 8-12 hours, mixed, and added with liquid paraffin and antioxidant at same time, extruded and granulated through a co-rotating twin-screw extruder, dried and subjected to injection molding to obtain final product.