• 专利标题:   Graphene-polypyrrole-gold nanoparticle composite material, comprises gold nanoparticle is supported on graphene-polypyrrole composite by combination of in-situ chemical polymerization and electrostatic adsorption.
  • 专利号:   CN108760855-A
  • 发明人:   ZOU Y, LIANG J, XIANG C, CHU H, QIU S, SUN L, XU F
  • 专利权人:   UNIV GUILIN ELECTRONIC TECHNOLOGY
  • 国际专利分类:   G01N027/30, G01N027/327
  • 专利详细信息:   CN108760855-A 06 Nov 2018 G01N-027/327 201902 Pages: 7 Chinese
  • 申请详细信息:   CN108760855-A CN10524155 28 May 2018
  • 优先权号:   CN10524155

▎ 摘  要

NOVELTY - A graphene-polypyrrole-gold nanoparticle composite material comprises gold nanoparticle is supported on a graphene-polypyrrole composite by a combination of in-situ chemical polymerization and electrostatic adsorption. USE - Graphene-polypyrrole-gold nanoparticle composite material. ADVANTAGE - The graphene-polypyrrole-gold nanoparticle composite material has lowest detection limit and high selectivity, in simple, cost effective and convenient manner. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a method for preparing a graphene-polypyrrole-gold nanoparticle composite material, which involves dissolving hydrochloric acid, pyrrole, graphene and water in the aqueous solution, dispersing graphene ultrasonically into the solution, which is recorded as solution M with ammonium persulfate and water meets a certain mass ratio, adding ammonium persulfate to the aqueous solution and recording as solution N, using mixed reaction of the solution to prepare a polypyrrole-graphene rice composite material, adding solution N dropwise to the solution M and stirring by a magnetic stirrer, after completing the dropwise addition, allowing the solution, reacting polypyrrole-graphene rice composite material for 2-4 hours, filtering, washing and drying, preparing gold nanoparticle solution with chloroauric acid, trisodium citrate, sodium borohydride and water in a certain mass ratio, adding chloroauric acid to water and stirring, adding trisodium citrate and adding sodium borohydride to obtain gold nanoparticle solution, adding the polypyrrole-graphene rice composite to the gold nanoparticle solution, stirring, filtering, washing and drying to obtain the finished product.