• 专利标题:   Phosphine compound, prepared by adding phosphorus trichloride, sublimed sulfur, aluminum trichloride, reactant, and tetrahydrofuran into reaction kettle, stirring, adding catalyst, heating and carrying out reflux reaction.
  • 专利号:   CN112645981-A
  • 发明人:   BAO Y, WENG S
  • 专利权人:   LUAN KOREDA NEW MATERIALS CO LTD
  • 国际专利分类:   B01J021/18, B01J023/80, B01J027/128, B01J027/138, B01J031/02, B01J032/00, B01J035/06, B01J037/02, B01J037/16, B01J037/34, C01B032/198, C07F009/50, D01F011/14
  • 专利详细信息:   CN112645981-A 13 Apr 2021 C07F-009/50 202142 Pages: 6 Chinese
  • 申请详细信息:   CN112645981-A CN11391198 01 Dec 2020
  • 优先权号:   CN11391198

▎ 摘  要

NOVELTY - Phosphine compound, prepared by adding phosphorus trichloride, sublimed sulfur, aluminum trichloride, reactant, and tetrahydrofuran into a reaction kettle, stirring at 0-3 degrees C for 20-30 minutes at a speed of 200-300 revolutions/minute, adding the catalyst, heating to 70-80 degrees C, and carrying out the reflux reaction for 3-8 hours, is claimed. USE - Used as phosphine compound. ADVANTAGE - The compound has good reduction effect and reductive carrier, is easy to recycle and the recovered catalyst can be treated with potassium borohydride and used again, which greatly reduces the preparation cost and reduces the waste of resources.