• 专利标题:   Preparation of oxidized graphene modified polymer cement waterproof coating involves mixing concentrated sulfuric acid, graphite powder and sodium nitrate mixture, cooling, mixing, adding potassium permanganate, and reacting.
  • 专利号:   CN106746965-A
  • 发明人:   WU H, ZHANG S
  • 专利权人:   CHAMPION CHEM YANGZHOU CO LTD
  • 国际专利分类:   C01B032/198, C04B111/27, C04B014/02, C04B028/00
  • 专利详细信息:   CN106746965-A 31 May 2017 C04B-028/00 201751 Pages: 5 Chinese
  • 申请详细信息:   CN106746965-A CN11071624 29 Nov 2016
  • 优先权号:   CN11071624

▎ 摘  要

NOVELTY - Preparation of oxidized graphene modified polymer cement waterproof coating involves mixing 50 pts. wt. concentrated sulfuric acid, 5 pts. wt. graphite powder and 5 pts. wt. sodium nitrate mixture, cooling at 10 degrees C, mixing, adding 16-20 pts. wt. potassium permanganate, reacting at 35 degrees C for 9 hours, heating to 80 degrees C for 1 hour, adding 600 pts. wt. deionized water and hydrogen peroxide, reacting, filtering, washing, adjusting pH to 7 using sodium hydroxide, ultrasonic treating for 2 hours, and mixing 106-352 pts. wt. filler, 1-3 pts. wt. defoamer and 1-3 pts. wt. preservatives. USE - Method for preparing oxidized graphene modified polymer cement waterproof coating (claimed). ADVANTAGE - The coating is durable, tough, and has high tensile strength and improved mechanical properties. DETAILED DESCRIPTION - Preparation of oxidized graphene modified polymer cement waterproof coating comprises mixing 50 pts. wt. concentrated sulfuric acid, 5 pts. wt. graphite powder and 5 pts. wt. sodium nitrate mixture, cooling at 10 degrees C, mixing, adding 16-20 pts. wt. potassium permanganate, reacting at 35 degrees C for 9 hours, heating to 80 degrees C for 1 hour, adding 600 pts. wt. deionized water and hydrogen peroxide, reacting, filtering, washing, adjusting pH to 7 using sodium hydroxide, ultrasonic treating for 2 hours, mixing 106-352 pts. wt. filler, 1-3 pts. wt. defoamer, 1-3 pts. wt. preservatives, 1-3 pts. wt. polycarboxylic acid water-reducing agent, 6-20 pts. wt. graphene solution and 100-332 pts. wt. acrylic polymer emulsion, adding 106-352 pts. wt. cement, stirring for 5-12 minutes, dissolving, and standing for 5 minutes.