• 专利标题:   Continuously producing graphene involves using two sections of tubular reactors for intercalation-micro oxidation reaction, mixing crystalline flake graphite with concentrated sulfuric acid in first section of tubular reactor, then adding potassium permanganate to perform secondary reaction.
  • 专利号:   CN115231563-A
  • 发明人:   WANG C, YIN J, GENG S, QIN H, YANG S, HAN M, ZHANG Y, LIU Y, YANG K
  • 专利权人:   UNIV QINGDAO SCI TECHNOLOGY
  • 国际专利分类:   C01B032/192
  • 专利详细信息:   CN115231563-A 25 Oct 2022 C01B-032/192 202294 Chinese
  • 申请详细信息:   CN115231563-A CN11017974 24 Aug 2022
  • 优先权号:   CN11017974

▎ 摘  要

NOVELTY - Continuously producing graphene involves using two sections of tubular reactors for intercalation-micro oxidation reaction, mixing crystalline flake graphite with concentrated sulfuric acid in the first section of the tubular reactor at low temperature for one time. The temperature of the two-section tube reactor is increased to a certain temperature, adding potassium permanganate, and performing the secondary reaction. The material of the dual-section pipe type reactor is pressurized by the pump, after heating by the fast heater, flashing the flash evaporator, and the gas phase goes to tail-removing processing system, after collecting the powder washing by acid washing for three times to obtain the product graphene. USE - Method for continuously producing graphene. ADVANTAGE - The method uses a tubular reactor as the main reactor, which ensures continuous process, is easy to realize automatic operation with low labor intensity and stable product quality. DESCRIPTION OF DRAWING(S) - The drawing shows a flow chart of a production process of a continuous production of graphene. (Drawing includes non-English language text). 1First section reactor 2Second section reactor 3Mixer 4Material pump 5Fast heater 6Throttle valve 7Flash tank