• 专利标题:   Method for preparing graphene/carbonized chromium composite nano material, involves dissolving chromium (III) nitrate nonahydrate in ethanol, adding mixed solution of complex graphene, drying followed by collecting and grinding.
  • 专利号:   CN105932309-A, CN105932309-B
  • 发明人:   LV H, NIE Z
  • 专利权人:   QINGDAO COWOO ENERGY TECHNOLOGY CO LTD
  • 国际专利分类:   B82Y030/00, H01M004/90
  • 专利详细信息:   CN105932309-A 07 Sep 2016 H01M-004/90 201670 Pages: 13 Chinese
  • 申请详细信息:   CN105932309-A CN10570623 19 Jul 2016
  • 优先权号:   CN10570623

▎ 摘  要

NOVELTY - A graphene/carbonized chromium composite nano material preparing method involves dissolving chromium (III) nitrate nonahydrate in anhydrous ethanol, adding graphite dilute solution and nano carbon black powder. Urea is dissolved in absolute alcohol at a mass ratio of 1:1-8. The mixture is added with obtained solution, the mixed solution of complex graphene is added into the sonicated solution, drying in oven. The dried sample is placed in the crucible of a tubular furnace and pyrolyzed, followed by continuing to raise the temperature, cooling, collecting and grinding to obtain product. USE - Method for preparing graphene/carbonized chromium composite nano material. DETAILED DESCRIPTION - A graphene/carbonized chromium composite nano material preparing method involves dissolving chromium (III) nitrate nonahydrate in anhydrous ethanol, adding graphite dilute solution and nano carbon black powder at ratio of 1: 5-10, ultrasonically dispersing at 75-80 degrees C for 10-30 min. Urea is dissolved in absolute alcohol at a mass ratio of 1:1-8 under the stirring of water at 75-80 degrees C. The mixture is added with obtained solution, where the molar ratio of chromium (III) nitrate nonahydrate and urea is 1:5-1, the mixed solution of complex graphene is added into the sonicated solution, drying in oven at 800 degrees C for 2-3 hours. The dried sample is placed in the crucible of a tubular furnace and pyrolyzed at 500-600 degrees C for 1-3 hours under nitrogen atmosphere, followed by continuing to raise the temperature to 800-1200 degrees C for 2-4 hours, natural cooling, collecting and grinding to obtain product.