• 专利标题:   Preparation of flexible graphene/permeable fiber composite microwave absorbing material by placing permeable fiber preform in muffle furnace, under air atmosphere, heat treating, cooling, and washing with acetone and deionized water.
  • 专利号:   CN106893550-A, CN106893550-B
  • 发明人:   YIN X, HAN M, SONG C
  • 专利权人:   UNIV NORTHWESTERN POLYTECHNICAL, UNIV NORTHWESTERN POLYTECHNICAL
  • 国际专利分类:   C09K003/00
  • 专利详细信息:   CN106893550-A 27 Jun 2017 C09K-003/00 201761 Pages: 7 Chinese
  • 申请详细信息:   CN106893550-A CN10098024 23 Feb 2017
  • 优先权号:   CN10098024

▎ 摘  要

NOVELTY - Preparation of flexible graphene/permeable fiber composite microwave absorbing material includes placing permeable fiber preform in a muffle furnace, under air atmosphere, heat treating, cooling, respectively washing with acetone and deionized water and drying, coating the surface of treated permeable fiber with graphene oxide aqueous solution, drying, repeating the coating step for multiple times, placing the graphene oxide-coated permeable fiber in a muffle furnace, heat treating under the protection of argon gas or nitrogen atmosphere, and forming graphene/fiber. USE - Preparation of flexible graphene/permeable fiber composite microwave absorbing material (claimed). ADVANTAGE - The method provides flexible graphene/permeable fiber composite microwave absorbing material, which has adjustable absorption frequency, minimum reflection loss of up to - 45 dB, reflection loss frequency width of less than 10 dB at 0-4.2 GHz, and stable electromagnetic wave absorbing property after bending. DETAILED DESCRIPTION - Preparation of flexible graphene/permeable fiber composite microwave absorbing material comprises placing permeable fiber preform in a muffle furnace, under air atmosphere, heat treating at 400-600 degrees C, keeping the temperature for 1-3 hours, cooling, respectively washing with acetone and deionized water and drying, coating the surface of treated permeable fiber with graphene oxide aqueous solution, drying at 40-80 degrees C, repeating the coating step for multiple times, placing the graphene oxide-coated permeable fiber in a muffle furnace, heat treating under the protection of argon gas or nitrogen atmosphere at 400-700 degrees C for 0.5-3 hours, forming graphene/fiber, vacuum impregnating with polydimethylsiloxane (PDMS) for 5-30 minutes, curing in drying box for 1-10 hours at 60-100 degrees C, and obtaining flexible reduction graphene/fiber composite material.