• 专利标题:   Preparing graphene aerogels loaded mesoporous lithium iron phosphate nanosheet complex comprises adding graphene oxide solution in a hydrothermal kettle, reacting, naturally cooling, freezing and drying.
  • 专利号:   CN106920931-A
  • 发明人:   ZHOU Y, LU J, TIAN X, JIANG T, TU X, HU M
  • 专利权人:   UNIV WUHAN SCI TECHNOLOGY
  • 国际专利分类:   B82Y030/00, H01M010/0525, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN106920931-A 04 Jul 2017 H01M-004/36 201756 Pages: 9 Chinese
  • 申请详细信息:   CN106920931-A CN10121699 02 Mar 2017
  • 优先权号:   CN10121699

▎ 摘  要

NOVELTY - Preparing graphene aerogels loaded mesoporous lithium iron phosphate nanosheet complex comprises (i) adding 1.5-5 kg/m3 graphene oxide solution in a hydrothermal kettle, reacting for 4-10 hours at 120-220 degrees C, naturally cooling, freezing and drying to obtain the graphene gas gel, (ii) mixing lithium source, phosphate source and iron source in the ratio of 1:1: 1-1.05, mixing the lithium iron phosphate nano sheet of the alkene gas gel loaded mesoporous lithium iron phosphate nano complex material and the graphene surface three-dimensional macro-pore gas gel to obtain the product. USE - The method is useful for preparing graphene aerogels loaded mesoporous lithium iron phosphate nanosheet complex (claimed). ADVANTAGE - The method is simple process, easy to operate and suitable for industrial production. DETAILED DESCRIPTION - Preparing graphene aerogels loaded mesoporous lithium iron phosphate nanosheet complex comprises (i) adding 1.5-5 kg/m3 graphene oxide solution in a hydrothermal kettle, reacting for 4-10 hours at 120-220 degrees C, naturally cooling, freezing and drying to obtain the graphene gas gel, (ii) mixing lithium source, phosphate source and iron source in the ratio of 1:1: 1-1.05, adding the lithium source into the de-ionized water, stirring, ultrasonically dispersing to obtain sol I, the concentration of the phosphate source is 0.1-2 mol/l, (iii) dripping the sol I to adsorption saturated at the graphene air gel surface, drying for 5-6 hours at room temperature, drying for 10-15 hours to obtain the precursor II at 50-55 degrees C, (iv) adding the precursor II in a tubular atmosphere furnace, calcining for 5-12 hours at 600-750 degrees C, cooling to obtain graphene gas gel loaded mesoporous lithium iron phosphate nano complex material, mixing the lithium iron phosphate nano sheet of the alkene gas gel loaded mesoporous lithium iron phosphate nano complex material and the graphene surface three-dimensional macro-pore gas gel to obtain the product.