• 专利标题:   Preparing graphene involves purifying graphene production waste water or/and concentrating, putting graphite in potassium permanganate and processing, uniformly mixing graphene production waste water, reacting and adding water to dilute.
  • 专利号:   CN108046248-A
  • 发明人:   LIANG Y, CHEN G, YANG Z, ZHU H
  • 专利权人:   GUANGDONG POLYROCKS CHEM CO LTD
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN108046248-A 18 May 2018 C01B-032/19 201839 Pages: 7 Chinese
  • 申请详细信息:   CN108046248-A CN11191420 24 Nov 2017
  • 优先权号:   CN11191420

▎ 摘  要

NOVELTY - Preparing graphene involves purifying graphene production waste water or/and concentrating, putting graphite in potassium permanganate and processing, uniformly mixing graphene production waste water, reacting at 0-100 degrees C for 10-240 minutes, adding water to dilute, continuously reacting for 1-15 minutes, and filtering to obtain filtrate and filter cake. The filter cake is washed by water, washing liquid is mixed with the filtrate to obtain production waste liquid. The filter cake, water and hydrogen peroxide solution are mixed and stirred for 1-15 minutes to obtain intercalated graphite. The intercalated graphite is separated out, dissolved in water, and then placed in the microwave reactor, protective gas is filled, reacted for 1-15 minutes to obtain graphene. The operation is repeated for 3-5 times. USE - Method for preparing graphene. ADVANTAGE - The method enables to prepare graphene that is suitable for large-scale popularization, has high yield and good quality, and reduces the production cost.