• 专利标题:   Preparation of nitrogen doped graphene composite lithium-iron-phosphate cathode material for lithium ion battery, involves dispersing graphite oxide in water and dispersing iron source, lithium source and phosphoric acid in water.
  • 专利号:   CN105514366-A, CN105514366-B
  • 发明人:   LI G, LIU W, XU H, REN M, YANG M, LI F
  • 专利权人:   UNIV QILU TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/58, H01M004/587
  • 专利详细信息:   CN105514366-A 20 Apr 2016 H01M-004/36 201659 Pages: 6 English
  • 申请详细信息:   CN105514366-A CN10877532 04 Dec 2015
  • 优先权号:   CN10877532

▎ 摘  要

NOVELTY - The preparation method of nitrogen doped graphene composite lithium-iron-phosphate cathode material involves uniformly dispersing graphite oxide in deionized water, adding nitrogen, stirring, dispersing iron source, phosphoric acid and lithium source in deionized water, stirring, obtaining uniform and stable dispersion liquid, mixing dispersion, stirring, drying in a freeze-dried condition, obtaining a solid mixture, precalcining the solid mixture under an inert gas atmosphere for 2-10 hours to obtain a reaction precursor and roasting the precursor under inert gas atmosphere. USE - Preparation of nitrogen doped graphene composite lithium-iron-phosphate cathode material for lithium ion battery. ADVANTAGE - The method prepares nitrogen doped graphene composite lithium-iron-phosphate cathode material by simple and short process at low cost. DETAILED DESCRIPTION - The preparation method of nitrogen doped graphene composite lithium-iron-phosphate cathode material (LiFePO4) involves uniform dispersing graphite oxide in deionized water, adding nitrogen, stirring for 1-10 hours, dispersing iron source, phosphoric acid and lithium source in deionized water, stirring, obtaining uniform and stable dispersion liquid, mixing dispersion, stirring for 10-48 hours, drying in a freeze-dried condition, obtaining a solid mixture, precalcining the solid mixture at 200-500 degrees C under an inert gas atmosphere for 2-10 hours to obtain a reaction precursor and roasting the precursor at 500-800 degrees C under inert gas atmosphere for 1-24 hours.