• 专利标题:   Preparation of graphene/copper composite material involves adding copper sulfate pentahydrate, nickel sulfate, citric acid, and boric acid to deionized water, stirring at room temperature to obtain mixed solution, and heating in water bath.
  • 专利号:   CN103736993-A, CN103736993-B
  • 发明人:   HU W, ZHANG Q, LIU D, LIU L, DENG Y, SHEN B, WU Z
  • 专利权人:   UNIV SHANGHAI JIAOTONG
  • 国际专利分类:   B22F001/02, B22F009/24, C23C018/40
  • 专利详细信息:   CN103736993-A 23 Apr 2014 B22F-001/02 201443 Pages: 7 Chinese
  • 申请详细信息:   CN103736993-A CN10002980 03 Jan 2014
  • 优先权号:   CN10002980

▎ 摘  要

NOVELTY - Graphene/copper composite material is prepared by adding copper sulfate pentahydrate, nickel sulfate, citric acid, and boric acid to deionized water, stirring at room temperature, heating in water bath while magnetically stirring, adding graphene oxide solution, mixing to obtain mixed solution, adding sodium hypophosphite solution, mixing to accelerate reaction, performing ultrasonic dispersion treatment, repeatedly filtering with microporous filtration membrane, washing with deionized water a number of times until pH is neutral, vacuum drying, and reducing under reducing atmosphere. USE - Preparation of graphene/copper composite material (claimed). ADVANTAGE - Graphene/copper composite material has stable dispersibility, and preparation is low-cost and easy to operate, has mild reaction conditions and high reduction degree and product quality, and uses non-toxic reducing agent and simple device. DESCRIPTION OF DRAWING(S) - The drawing shows a transmission electron microscope image of graphene/copper composite material.