• 专利标题:   Preparation of iron oxide/nitrogen-doped graphene material used for lithium ion battery cathode involves preparing polydopamine/graphene material, reacting with iron salt precursor, adding sodium hydroxide, washing, drying, and heating.
  • 专利号:   CN107910515-A
  • 发明人:   ZHANG X, FAN Q, YANG H, MI P, MA S
  • 专利权人:   UNIV DALIAN TECHNOLOGY
  • 国际专利分类:   H01M004/36, H01M004/52, H01M004/62, H01M010/0525, B82Y030/00
  • 专利详细信息:   CN107910515-A 13 Apr 2018 H01M-004/36 201830 Pages: 7 Chinese
  • 申请详细信息:   CN107910515-A CN11083222 07 Nov 2017
  • 优先权号:   CN11083222

▎ 摘  要

NOVELTY - Preparation of iron oxide/nitrogen-doped graphene material involves adding dopamine hydrochloride to graphene oxide and hydrochloric acid at mass ratio of 1:0.5-1:5, adding trihydroxymethyl aminomethane to adjust pH to 8.5, reacting for 12-24 hours at room temperature, filtering, eluting with deionized water to neutral, and drying at 80 degrees C for 12 hours; and dispersing in iron salt precursor aqueous solution at mass ratio of 1:3-1:10, adding iron salt, adding 1 mol/L sodium hydroxide solution reacting at room temperature to 50 degrees C for 12-24 hours, filtering, and washing. USE - Method for preparing iron oxide/nitrogen-doped graphene material used for lithium ion battery cathode (claimed). ADVANTAGE - The lithium battery has excellent lithium properties. DETAILED DESCRIPTION - Preparation of iron oxide/nitrogen-doped graphene material comprises adding dopamine hydrochloride to graphene oxide and hydrochloric acid at mass ratio of 1:0.5-1:5, adding trihydroxymethyl aminomethane to adjust pH to 8.5, reacting for 12-24 hours at room temperature, filtering, eluting with deionized water to neutral, and drying at 80 degrees C for 12 hours; dispersing in iron salt precursor aqueous solution at mass ratio of 1:3-1:10, adding iron salt, adding 1 mol/L sodium hydroxide solution reacting at room temperature to 50 degrees C for 12-24 hours, filtering, washing by deionized water to neutral, and drying at 80 degrees C for 12 hours; and heating to 400-500 degrees C under protection of inert gas for 1-3 hours.