• 专利标题:   Preparation of sulfonated graphene/polyaniline composite material used as mercury ion absorbent in mercury ion containing wastewater, by subjecting water and natural graphite to chemical oxidization, and adding ammonium persulfate.
  • 专利号:   CN102702517-A
  • 发明人:   HU J, LI L, LV S, YAN H, ZHENG H, YU X
  • 专利权人:   WUHAN INST TECHNOLOGY
  • 国际专利分类:   B01J020/26, C02F001/28, C08G073/02, C08K003/04, C08K009/00, C08L079/02
  • 专利详细信息:   CN102702517-A 03 Oct 2012 C08G-073/02 201304 Pages: 8 Chinese
  • 申请详细信息:   CN102702517-A CN10188010 08 Jun 2012
  • 优先权号:   CN10188010

▎ 摘  要

NOVELTY - A sulfonated graphene/polyaniline composite material is prepared by subjecting natural graphite to chemical oxidization to obtain sulfonated graphene, dispersing in water to obtain sulfonated graphene aqueous solution (2 mg/ml), adding aniline (0.02-0.5 mol/l), mixing to obtain solution A, dissolving ammonium persulfate in hydrochloric acid at a mole ratio of 0.5-2:1, adding obtain solution to solution A, stirring for 6-24 hours, filtering, washing the filter cake until the washing solution is colorless, and vacuum drying. USE - Method of preparing a sulfonated graphene/polyaniline composite material for use as mercury ion absorbent in mercury ion containing wastewater (claimed). ADVANTAGE - The method is low cost, and has good absorption performance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method of using the sulfonated graphene/polyaniline composite material as mercury ion absorbent in mercury ion containing wastewater comprising adding composite material (10-70 mg) to wastewater (30 ml) having mercury ion content of 30-60 mg/l, reacting for 0.5-120 hours, and adjusting pH value of wastewater to 4-8.