• 专利标题:   Producing graphene-coated inorganic particles, comprises e.g. preparing first mixed solution by introducing inorganic particle into surface treatment solution containing coupling agent, agitating, filtering, drying, and preparing second mixed solution.
  • 专利号:   KR2361553-B1
  • 发明人:   SONG H, KYOUNGJEONGBAE
  • 专利权人:   ELEMENT CO LTD KB
  • 国际专利分类:   B22F001/00
  • 专利详细信息:   KR2361553-B1 14 Feb 2022 B22F-001/00 202217 Pages: 12
  • 申请详细信息:   KR2361553-B1 KR154845 18 Nov 2020
  • 优先权号:   KR154845

▎ 摘  要

NOVELTY - A first mixed solution is prepared by introducing inorganic particles into a surface treatment solution containing a coupling agent, and is agitated. The first mixed solution is filtered and mixture is dried to obtain inorganic particles having a functional group bound to surface. The surface-treated inorganic particle is injected into a solution containing non-oxidized graphene to obtain a second mixed solution, and second mixed solution is stirred. The non-oxidized graphene has an ID/IG value of 0.16-0.23 or less, which is ratio of D peak intensity (ID) to G peak intensity (IG) in Raman spectrum measurement result, and oxygen content is 0.001-1 at.% or less. The coupling agent is 3-aminopropyl triethoxy silane (APTES), 3-glycidoxypropyl trimethoxysilane, Triton X-100 (RTM: Nonionic surfactant) (2-(4-(2,4,4-trimethylpentan-2-yl)phenoxy) ethanol) and/or polyvinyl acetate (PVA). The surface treatment solution includes solvent, i.e. deionized water, ethanol and/or acetic acid. USE - The method is useful for producing graphene-coated inorganic particles. ADVANTAGE - The graphene-coated inorganic particles exhibit excellent thermal conductivity by minimizing structural defects and damage to inorganic particles during graphene coating. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene-coated inorganic particles manufactured by above method.