• 专利标题:   Method for preparing reduced graphene oxide/polypyrrole/filter paper composite flexible electrode material, involves cutting filter paper into desired shape and immersing filter paper in aqueous solution of ferric chloride.
  • 专利号:   CN109003840-A
  • 发明人:   MA M, MA C, CAO W, LIU S, LI Z, WANG B, BIAN J
  • 专利权人:   UNIV BEIJING FORESTRY
  • 国际专利分类:   H01G011/86, H01G011/24, H01G011/36, H01G011/48
  • 专利详细信息:   CN109003840-A 14 Dec 2018 H01G-011/86 201912 Pages: 14 Chinese
  • 申请详细信息:   CN109003840-A CN10903566 09 Aug 2018
  • 优先权号:   CN10903566

▎ 摘  要

NOVELTY - The reduced graphene oxide/polypyrrole/filter paper composite flexible electrode material preparing method involves cutting a filter paper into a desired shape, immersing the filter paper in an aqueous solution of ferric chloride for 30 minutes and taking out and draining in a refrigerator. The immersed filter paper is immersed in an isopropanol solution having a concentration of 1-2 vol.% pyrrole monomer for 24 hours to obtain product. The product is taken out and drained, washed with deionized water and vacuum-dried at room temperature for 24 hours to obtain dried product. The dried product is immersed in a graphene dispersion having a concentration of 0.16-2.4 mg/L for 1-3 hours and an equal volume of 0.1-0.2 mol/L is added to the mixture of ascorbic acid solution and stirred for 12 hours, followed by taking out and draining the product, washing with deionized water and vacuum-drying at room temperature for 24 hours to obtain the finished product. USE - Method for preparing reduced graphene oxide/polypyrrole/filter paper composite flexible electrode material. ADVANTAGE - The method enables preparing reduced graphene oxide/polypyrrole/filter paper composite flexible electrode material with excellent energy storage potential and high specific capacitance, in flexible and cost effective manner. DETAILED DESCRIPTION - The reduced graphene oxide/polypyrrole/filter paper composite flexible electrode material preparing method involves cutting a filter paper into a desired shape, immersing the cutted filter paper in an aqueous solution of ferric chloride having a molar concentration of 0.1-0.5 mol/L for 30 minutes and taking out and draining in a refrigerator for 4 degrees C. The immersed filter paper is immersed in an isopropanol solution having a concentration of 1-2 vol.% pyrrole monomer for 24 hours to obtain product. The product is taken out and drained, washed with deionized water and vacuum-dried at room temperature for 24 hours to obtain dried product. The dried product is immersed in a graphene dispersion having a concentration of 0.16-2.4 mg/L for 1-3 hours and an equal volume of 0.1-0.2 mol/L is added to the mixture of ascorbic acid solution and stirred for 12 hours, followed by taking out and draining the product, washing with deionized water and vacuum-drying at room temperature for 24 hours to obtain the finished product. An INDEPENDENT CLAIM is also included for a reduced graphene oxide/polypyrrole/filter paper composite flexible electrode material prepared by the method.