• 专利标题:   Preparation of graphene fiber for use in e.g. energy storage device, involves dispersing oxidized graphene in deionized water, mixing uniformly dispersed aqueous solution of graphene oxide with chloroacetic acid, heating and cooling.
  • 专利号:   CN105887244-A, CN105887244-B
  • 发明人:   YANG Y
  • 专利权人:   SUZHOU YUXI NEW MATERIAL TECHNOLOGY CO, SUZHOU YUXI NEW MATERIAL TECHNOLOGY CO
  • 国际专利分类:   C01B031/04, D01F009/12, C01B032/184
  • 专利详细信息:   CN105887244-A 24 Aug 2016 D01F-009/12 201673 Pages: 4 Chinese
  • 申请详细信息:   CN105887244-A CN10474260 27 Jun 2016
  • 优先权号:   CN10474260

▎ 摘  要

NOVELTY - Preparation of graphene fiber involves (i) ultrasonically dispersing oxidized graphene in deionized water to obtain aqueous solution of uniformly dispersed graphene oxide, (ii) mixing uniformly dispersed aqueous solution of graphene oxide with chloroacetic acid, heating under stirring condition, maintaining for 0.5-3 hours, then cooling to room temperature and filtering, drying to obtain carboxylated graphene oxide, (iii) dispersing carboxylated graphene in N,N-dimethylformamide to obtain a spinning dope, carrying out wet spinning to prepare graphene fiber. USE - Preparation of graphene fiber for use in energy storage device, photovoltaic devices and sensors. ADVANTAGE - The graphene fiber is prepared by a simple method. The method is easy to industrialization. The prepared graphene fiber has excellent conductivity and high flexibility. DETAILED DESCRIPTION - Preparation of graphene fiber involves (i) ultrasonically dispersing oxidized graphene in deionized water to obtain aqueous solution of uniformly dispersed graphene oxide, (ii) mixing uniformly dispersed aqueous solution of graphene oxide with chloroacetic acid, heating at 60-80 degrees C under stirring condition, maintaining for 0.5-3 hours, then cooling to room temperature and filtering with a filter, drying to obtain carboxylated graphene oxide, (iii) dispersing carboxylated graphene in N,N-dimethylformamide to obtain a spinning dope, carrying out wet spinning to prepare graphene fibers having electrical conductivity of 2.0-2.2/asterisk104 S/m.