• 专利标题:   Preparation of yellow-green fluorescence graphene quantum dot used for, e.g. sense analysis, by adding nitric acid and sulfuric acid to graphene oxide solution, mixing, subjecting mixture to microwave treatment, and cooling.
  • 专利号:   CN102602924-A, CN102602924-B
  • 发明人:   JI J, LI L, ZHU J
  • 专利权人:   UNIV NANJING
  • 国际专利分类:   C01B031/04, C09K011/65
  • 专利详细信息:   CN102602924-A 25 Jul 2012 C01B-031/04 201322 Pages: 7 Chinese
  • 申请详细信息:   CN102602924-A CN10107483 13 Apr 2012
  • 优先权号:   CN10107483

▎ 摘  要

NOVELTY - A yellow-green fluorescence graphene quantum dot is prepared by adding (ml/15 mg of graphene oxide) nitric acid (8-16) having a concentration of 65-68% and sulfuric acid (2-4) having a concentration of 98% to a graphene oxide solution, mixing, subjecting mixture to microwave treatment at a power of 240-800 W for 3-5 hours, cooling to room temperature, adjusting pH value to 8, filtering using micropore membrane, and conducting dialysis. USE - Method of preparing a yellow-green fluorescence graphene quantum dot for use in living beings marking or sense analysis. ADVANTAGE - The method prepares product having good dispersibility in water, long useful life, and good fluorescence quality.