• 专利标题:   Preparing metal oxide nano particles loaded three-dimensional graphene material comprises e.g. preparing homogeneous blend of metal organic compound and benzoxazine monomer, heating for cross-linking and irradiating with laser.
  • 专利号:   CN113060721-A, CN113060721-B
  • 发明人:   LIU X, YU W, ZHAO W
  • 专利权人:   NINGBO INST MATERIALS TECHNOLOGY ENG C
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B013/18, C01B032/184, C01G023/053, C01G037/02, C01G039/02, C01G049/08, C01G051/04, C01G053/00, C01G053/04, H01G011/46
  • 专利详细信息:   CN113060721-A 02 Jul 2021 C01B-032/184 202171 Pages: 19 Chinese
  • 申请详细信息:   CN113060721-A CN10274685 15 Mar 2021
  • 优先权号:   CN10274685

▎ 摘  要

NOVELTY - Preparing metal oxide nano particles loaded three-dimensional graphene material comprises mixing metal organic compound and benzoxazine monomer, heating to above the melting point of the benzoxazine monomer, so as to achieve a homogeneous blend of the metal organic compound and the benzoxazine monomer to obtain a mixture; heating the mixture to above the curing temperature of the benzoxazine monomer and cross-linking and curing the benzoxazine monomer to form a metal organic compound/benzoxazine resin composite material; irradiating the metal organic compound/benzoxazine resin composite material with a laser, thus converting the metal organic compound/benzoxazine resin composite material into corresponding final product. USE - The metal oxide nano particles loaded three-dimensional graphene material is useful in energy storage, electrocatalysis, electromagnetic shielding material preparation and capacitor electrode material preparation fields (claimed). ADVANTAGE - The method: has simple process, short production period, low cost and no solvent. The metal oxide nano-particle loaded three-dimensional graphene material: exhibits extremely excellent comprehensive performance; has excellent application potential in the fields of energy storage, electromagnetic shielding and electrocatalysis. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for metal oxide nanoparticle-loaded three-dimensional graphene material prepared by above method, comprising a graphene framework material with a three-dimensional porous network structure and nano-sized metal oxide nanoparticles, where the metal oxide nanoparticles are uniformly distributed and embedded in the three-dimensional porous network structure of the graphene framework material, the loading amount of the metal oxide nanoparticles in the three-dimensional graphene material is 0.1-11.2 wt.%.