• 专利标题:   Preparation of two-dimensional graphene, by ultrasonically-dispersing layered material in solvent to obtain graphene dispersion, adding titanium oxide, rapidly-shearing to obtain crude product, distilling, washing and drying.
  • 专利号:   CN106115673-A
  • 发明人:   ZHANG Y, HUANG J
  • 专利权人:   ANHUI SANGRUISI ENVIRONMENTAL PROTECTION
  • 国际专利分类:   C01B019/04, C01B021/064, C01B031/04, C01G027/00, C01G033/00, C01G039/06, C01G041/00
  • 专利详细信息:   CN106115673-A 16 Nov 2016 C01B-031/04 201704 Pages: 4 Chinese
  • 申请详细信息:   CN106115673-A CN10467287 24 Jun 2016
  • 优先权号:   CN10467287

▎ 摘  要

NOVELTY - Preparation of two-dimensional graphene involves ultrasonically-dispersing a layered material in 10-20% solvent to obtain graphene dispersion, adding titanium oxide, adjusting pH value of the reaction mixture to less than 7, rapidly-shearing at 30-50 degrees C to obtain crude product, leaving crude product to stand still at -25 degrees C to -10 degrees C for 1-2 hours, distilling under reduced pressure, washing and drying at 90-170 degrees C. USE - Preparation of two-dimensional graphene (claimed).