• 专利标题:   Preparation of tin powder modified high stability nitrogen-doped graphene quantum dot includes mixing citric acid and urea in deionized water, performing ultrasonic dispersion treatment, heating, cooling, washing, shaking and standing.
  • 专利号:   CN109052375-A
  • 发明人:   ZHAO H, XIE H, WANG Y, LU G
  • 专利权人:   JIANGSU ANNATAI ENVIRONMENTAL TECHNOLOGY
  • 国际专利分类:   C01B032/184, B82Y030/00, C09K011/65
  • 专利详细信息:   CN109052375-A 21 Dec 2018 C01B-032/184 201922 Pages: 8 Chinese
  • 申请详细信息:   CN109052375-A CN11167991 08 Oct 2018
  • 优先权号:   CN11167991

▎ 摘  要

NOVELTY - Preparation of tin powder modified high stability nitrogen-doped graphene quantum dot comprises mixing citric acid and urea in deionized water at 1:3, adding reducing agent tin powder, performing ultrasonic dispersion treatment for 30 minutes, transferring to reaction vessel of PTFE high-temperature reaction chamber, sealing, heating in oven to 180 degrees C for 4 hours, cooling to room temperature, washing orange-yellow stable liquid with ethanol, shaking for 20 minutes and standing for 24 hours to remove other excess organic matter. USE - Method of preparing tin powder modified high stability nitrogen-doped graphene quantum dot. ADVANTAGE - The quantum dot has good purity, small particle size and uniform scale distribution and is conducive.