• 专利标题:   Manufacturing graphene, comprises removing hydrogen, nitrogen and oxygen content from graphite granule, crushing with metal components and sulfur, performing heat treatment, mixing gas-doped powder and carrying out ultrasonic treatment.
  • 专利号:   KR2013139461-A
  • 发明人:   GYEONG L H
  • 专利权人:   GYEONG L H
  • 国际专利分类:   B01J019/10, B01J002/08, C01B031/02, C01B031/04
  • 专利详细信息:   KR2013139461-A 23 Dec 2013 C01B-031/02 201410 Pages: 4
  • 申请详细信息:   KR2013139461-A KR062463 12 Jun 2012
  • 优先权号:   KR062463

▎ 摘  要

NOVELTY - Manufacturing pure graphene removing 96-99.9% of hydrogen, nitrogen and oxygen content from natural graphite granule or synthetic graphite granule; crushing the obtained graphite granule with metal components and sulfur using ball mill process; performing heat treatment on the crushed powder in the presence of gas; mixing gas-doped graphite powder in solvent and water; stirring using a rod; carrying out ultrasonic treatment to obtain separating gel composed of dispersed graphene; and removing solvent from the graphene. USE - The method is useful for manufacturing graphene (claimed). ADVANTAGE - The method is capable of manufacturing high yield of graphene with high purity. DETAILED DESCRIPTION - Manufacturing pure graphene removing 96-99.9% of hydrogen, nitrogen and oxygen content from natural graphite granule or synthetic graphite granule; crushing the obtained graphite granule with metal components and sulfur using ball mill process; performing heat treatment on the crushed powder in the presence of iodine, carbon dioxide, hydrogen, oxygen, carbon monoxide, nitrogen, helium, neon, argon, krypton, xenon, florine and chlorine at 120-180 degrees C; mixing gas-doped graphite powder in solvent comprising N-Methylpyrrolidone solvent, dimethylformamide solvent or alcohol and water; stirring using a rod; carrying out ultrasonic treatment to obtain separating gel composed of dispersed graphene; and removing solvent from the graphene.