• 专利标题:   High energy density graphene aerogel preparation involves mixing water and acid-containing graphene oxide dispersion under ultrasonication to prepare acid-free graphite oxide by using modified Hummers method.
  • 专利号:   CN108178146-A
  • 发明人:   SHAO J, TANG X
  • 专利权人:   UNIV GUIZHOU
  • 国际专利分类:   C01B032/184, C01B032/23
  • 专利详细信息:   CN108178146-A 19 Jun 2018 C01B-032/184 201853 Pages: 13 Chinese
  • 申请详细信息:   CN108178146-A CN10105127 02 Feb 2018
  • 优先权号:   CN10105127

▎ 摘  要

NOVELTY - High energy density graphene aerogel preparation involves mixing water and an acid-containing graphene oxide dispersion under ultrasonication to prepare acid-free graphite oxide by using modified Hummers method. The prepared pure graphite oxide is added to water to obtain a graphene oxide dispersion. The obtained acid-containing graphene oxide dispersion and the obtained graphene oxide dispersion are separately placed in a reaction vessel to carry out water under thermal reaction conditions to obtain columnar graphene hydrogel. The obtained columnar graphene hydrogels are placed in liquid nitrogen for freezing for 5-30 minutes, and then placed in a lyophilizer to freeze-dry to obtain the graphene aerogel. USE - Method for preparing high energy density graphene aerogel. ADVANTAGE - The method prepares the high energy density graphene aerogel in a simple, cost-effective and eco-friendly manner with high efficiency and controllable conditions. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic view of the scanning electron micrograph of the prepared graphene aerogel.