• 专利标题:   Graphene/black phosphorus nanosheet/sulfur-containing ionic liquid composite aerogel comprises graphene three-dimensional framework, black phosphorus nanosheet, and sulfur-containing ionic liquid.
  • 专利号:   CN107416846-A
  • 发明人:   ZHANG H, XING C, ZHANG J
  • 专利权人:   UNIV SHENZHEN
  • 国际专利分类:   B01J013/00, C01B017/00, C01B025/00, C01B032/198, C01B033/158
  • 专利详细信息:   CN107416846-A 01 Dec 2017 C01B-033/158 201804 Pages: 23 Chinese
  • 申请详细信息:   CN107416846-A CN11244939 29 Dec 2016
  • 优先权号:   CN11244939

▎ 摘  要

NOVELTY - A graphene/black phosphorus nanosheet/sulfur-containing ionic liquid composite aerogel comprises a graphene three-dimensional framework, a black phosphorus nanosheet, and a sulfur-containing ionic liquid supported on graphene three-dimensional framework. The black phosphorus nanosheet is surrounded by the sulfur-containing ionic liquid. The graphene/black phosphorus nanosheet/sulfur-containing ionic liquid composite aerogel has a three-dimensional porous network structure. USE - Graphene/black phosphorus nanosheet/sulfur-containing ionic liquid composite aerogel (claimed). ADVANTAGE - The graphene/black phosphorus nanosheet/sulfur-containing ionic liquid composite aerogel has high elasticity, recoverability, conductivity and stability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of graphene/black phosphorus nanosheet/sulfur-containing ionic liquid composite aerogel, which involves: (1) mixing solution containing black phosphorus nanosheet and sulfur-containing ionic liquid and graphene oxide aqueous solution, and uniformly mixing and stirring with reducing agent to obtain mixed solution; (2) carrying out heating on mixed solution under water bath and oxygen-free condition at 75-100 degrees C, and reacting for 1-3 hours to obtain graphene/black phosphorus nanosheet/sulfur-containing ionic liquid composite wet gel; and (3) sequentially placing graphene/black phosphorus nanosheet/sulfur-containing ionic liquid composite wet gel in a hydrophilic organic solvent and water for purification, and then carrying out freeze-drying to obtain product.