• 专利标题:   Preparing millimeter-scale core-shell structure sphere material involves feeding polystyrene foam balls into rotary drum, adjusting working temperature of rotary drum, and adding low-density material into rotary drum.
  • 专利号:   CN113621168-A, CN113621168-B
  • 发明人:   DENG Z, ZENG J, YANG Y, XU Z, LI S, WU W, ZHANG H, LI H, WANG H, DAI Z, YI J, TANG B, CAO M
  • 专利权人:   UNIV JIAXING
  • 国际专利分类:   C09D175/04, C09D167/06, C09D163/00, C08K003/04, C08K007/14, C08K007/06, C08K007/28, C08L025/06, C08J009/36
  • 专利详细信息:   CN113621168-A 09 Nov 2021 C08J-009/36 202104 Chinese
  • 申请详细信息:   CN113621168-A CN11061699 10 Sep 2021
  • 优先权号:   CN11061699

▎ 摘  要

NOVELTY - Preparing millimeter-scale core-shell structure sphere material involves feeding 5-10 pts. wt. polystyrene foam balls into a rotary drum, adjusting the working temperature of the rotary drum to 50-60degrees Celsius, adding 0.1-1 pts. wt. low-density material into the rotary drum, and uniformly mixing to obtain a first mixed spherical material, uniformly mixing 10 pts. wt. epoxy resin, 1 pts. wt. reactive diluent, 0.1 pts. wt. coupling agent and 1-4 pts. wt. amine curing agent to obtain a bottom shell coating, spraying the bottom shell coating on the surface of the first mixed spherical material by a spray gun to obtain a first core-shell structure spherical material, adjusting the working temperature of the rotary drum to room temperature, continuously adding 0.1-1 pts. wt. low-density material and 3-5 pts. wt. chopped fibers into the rotary drum to obtain a second mixed spherical material. USE - Method for preparing millimeter-scale core-shell structure sphere material. ADVANTAGE - The millimeter-scale core-shell sphere material has low energy consumption, low density, high strength and high yield, and improves the productivity and yield of millimeter-level core-shell sphere materials, and also has low density technical effect and high strength comprehensive performance. DETAILED DESCRIPTION - Preparing millimeter-scale core-shell structure sphere material involves feeding 5-10 pts. wt. polystyrene foam balls into a rotary drum, adjusting the working temperature of the rotary drum to 50-60degrees Celsius, adding 0.1-1 pts. wt. low-density material into the rotary drum, and uniformly mixing to obtain a first mixed spherical material, uniformly mixing 10 pts. wt. epoxy resin, 1 pts. wt. reactive diluent, 0.1 pts. wt. coupling agent and 1-4 pts. wt. amine curing agent to obtain a bottom shell coating, spraying the bottom shell coating on the surface of the first mixed spherical material by a spray gun to obtain a first core-shell structure spherical material, adjusting the working temperature of the rotary drum to room temperature, continuously adding 0.1-1 pts. wt. low-density material and 3-5 pts. wt. chopped fibers into the rotary drum to obtain a second mixed spherical material, then uniformly mixing 10 pts. wt. unsaturated polyester resin, 0.1-0.4 pts. wt. curing agent, 0.1 pts. wt. accelerator and 0.05 pts. wt. coupling agent to obtain a middle-layer shell coating, spraying the middle-layer shell coating on the surface of the second mixed spherical material through a spray gun to obtain a second core-shell structure spherical material and uniformly mixing 10 pts. wt. macromolecular polyol and 2-4 pts. wt. polyisocyanate curing agent to obtain a top shell coating, and spraying the top shell coating on the surface of the second core-shell structure spherical material by using a spray gun.