• 专利标题:   Preparing graphene oxide fibers by wet spinning comprises preparing graphene oxide mixtures in solvent selected from water, N-methyl-2-pyrrolidone, N,N-dimethyl formamide, and (f) injecting graphene oxide mixtures through nozzle into coagulation bath to obtain product.
  • 专利号:   WO2022265586-A1
  • 发明人:   JOMPHOAK A, JARUWONGRUNGSEE K, NUNTAWONG N, POGFAY T, WAIWIJIT U, MATUROS DANIELS T, JARIYAKUN K, PONGSAKSAWAD W, KHAMSUK P
  • 专利权人:   NAT SCI TECHNOLOGY DEV AGENCY
  • 国际专利分类:   C01B032/198, D01D001/09, D01D010/06, D01D005/08, D01F009/12
  • 专利详细信息:   WO2022265586-A1 22 Dec 2022 C01B-032/198 202305 Pages: 16 English
  • 申请详细信息:   WO2022265586-A1 WOTH000023 15 Jun 2022
  • 优先权号:   TH1003685

▎ 摘  要

NOVELTY - Method for preparing graphene oxide fibers by wet spinning, comprises (a) preparing graphene oxide mixtures in solvent chosen from water, N-methyl-2-pyrrolidone, and/or N,N-dimethyl formamide, which the concentration of graphene oxide of 5-30 mg/ml, and (b) injecting the graphene oxide mixtures obtained from step (a) through a nozzle with a diameter of 0.5-1.5 mm at a speed of 0.1-0.5 ml/minute into a coagulation bath rotated at 5-30 rpm to obtain graphene oxide fibers, where the coagulation bath comprises a coagulant of a silver nitrate in a solvent mixture of ethanol and water with a volumetric ratio of ethanol to water of 1:1-1:5, and the concentrations of silver nitrate solution is 0.1-0.5 Molar. USE - The method is used for preparing graphene oxide fibers by wet spinning. ADVANTAGE - The method prepares graphene oxide fibers by wet spinning technique using a coagulant to fabricate graphene oxide fibers with consistent length that can maintain their shape continuously without the use of additives while sustaining good electrical conductivity.